ACUAN STANDAR INTERNAL GEOKIMIA DENGAN MATRIKS STREAM SEDIMENTS WILAYAH SOREANG, JAWA BARAT
DOI:
https://doi.org/10.33332/jgsm.geologi.v23i1.95Abstract
Certified reference materials are needed in producing a good validity level of measurement process. The closer analytical result of CRM to its certificated value, the better quality of measurement would be. This studi was aimed to produce internal reference material in three kinds of stream sediment matrixes: the first is considered as natural stream sediment, the second suggest to be affected by industrial and anthropogenic actifity, and the last one was taken near by conventional gold mining location. All about sampling location, geological setting and megascopic description of the samples had been collected and saved properly. The three stream sediments samples were homogenized manually and separated in to some split bottles and were prepared and analyzed chemically to show their homogeneity. An Atomic Absorbance Spectrometry and X-Ray Floresence are used to analyze the samples for tatally nine times. Measurement results show that these in-house reference materials are in good level of homogeneity and many chemical elements can be used as a reference value with coefficient of variance <5%. Several factors influence the type of sediment are also reflected in the value of the elements content of each sample, where each example shows the content of the element in accordance with the factors that affect the flow of sediment respectively. This study could be continued further to produce a national reference material in stream sediments matrix.
Key words: : in–house reference material, stream sediments, AAS, XRF
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References
Anwar, I. 2003. Dasar-dasar Statistika. ALFABETA. Bandung.
Alzwar, M., Akbar, N., dan Bachri, S. 1992. Peta Geologi Lembar Garut dan Pameungpeuk, Jawa, Skala 1:100.000. Pusat Penelitian dan Pengembangan Geologi, Bandung.
Ayodele, O.S., 2011. Stream Sediment Geochemical Survey of Ara, Epe and Ijero Area, South Western Nigeria. International Journal of Science and Technology, v.1(6), h. 269-274.
Beaty, R.D., dan Kerber, J.D., 1993. Concept, Instrumentation dan Techniques in Atomic Absorption Spectrophotometry, 2nd edition. The Perkin-Elmer Corporation, Norwalk, CT, Amerika Serikat
Da Costa, A.C., Bigham, J.M., Rhoton, F.E., Traina, S.J., 1999. Quantification and Characterization of Maghemite in Soils Derived From Volcanic Rocks in Southern Brazil. Clays and Clay Mineral, v.47 (4), h.466 – 473.
Deines, P., Goldstein, P., Oelkers, S.L., Rudnick, E.H., Walter, R.L., 2003. Standards for publication of isotope ratio and chemical data in Chemical Geology. Chemical Geology, v. 202 (1-2), h. 1-4.
Flecther, W.K., 1997. Stream Sediment Geochemistry in Today's Exploration World. Proceedings of Exploration 97: Fourth Decennial International Conference on Mineral Exploration. h. 249 – 260.
Irzon, R., 2010. Pengujian Trace-Rare Earth Elements Terhadap AGV-2 dan GBW-07113 dengan ICP-MS. Kumpulan Makalah Sarana Teknik Pusat Survei Geologi, v.39, h. 51-66.
Irzon, R., Maryanto, S., dan Kurnia, 2011. Geokimia Batuan Sedimen Wilayah Muaradua, Sumatera Selatan pada Pembuatan Materi Acuan Standar Kimia Elemen. Kumpulan Makalah Sarana Teknik Pusat Survei Geologi, v.40, h. 67-79.
Karadjova, I., Izgi, B., Gucer, S., 2002. Fractionation and speciation of Cu, Zn and Fe in wine samples by atomic absorption spectrometry. Spectrochimica Acta, Part B 57, h. 581–590
Kind, M., 2002. Colloidal Aspects of Precipitation Processes. Chemical Engineering Science, v. 57, h. 4287 – 4293.
Lozano, R. dan Bernal, J.P., 2005. Characterization of a new set of eight geochemical reference materials for XRF major and trace element analysis. Revista Mexicana de Ciencias Geológicas, v. 22, núm. 3, h. 329-344
Nyakairu, G.W.A., Koeberl, C., 2001. Mineralogical and chemical composition and distribution of rare earth elements in clay-rich sediments from central Uganda. Geochemical Journal, vol. 35, h. 13 – 28.
Rollinson, H., 1993. Using Geochemical Data: evaluation, presentation, interpretation. Pearson Education Limited. Inggris.
Silitonga P.H., 2003. Peta Geologi Lembar Bandung, Jawa, Skala 1: 100.000. Pusat Penelitian dan Pengembangan Geologi, Bandung.
Siregar, D.A., Kurnia dan Irzon, R., 2012. Pengembangan Metode Analisis Zn Terhadap SNI 13-6974-2003 (Analisis Cu,Pb, Zn, Fe, Mn dan Cd Dalam Batuan Sulfida). Pertemuan dan Presentasi Ilmiah Standarisasi November 2012. Badan Standarisasi Nasional, h. 109-119
Sukiyah, E., Haryanto, A.D., dan Zakaria, Z., 2004. Aplikasi Sistem Informasi dalam Penetapan Kawasan Rawan Banjir di Kabupaten Bandung Bagian Selatan. Bulletin of Scientific Contribution, Volume 2 (1). h. 26-37
Sudjana, 1997. Metoda Statistika. Penerbit Tarsito. Edisi ke-6. Bandung
Tellinghuisen, J., 2008. Least Squares with non-normal data: estimating experimental variance functions. Analyst, v.133, h. 161 – 166.
Yamamoto, K., Yamashita, F., dan Adachi, M., 2005. Precise Determination of REE for Sedimentary Reference Rocks Issued by The Geological Survey of Japan. Geochemical Journal, v.39, h. 289 – 297.
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